Resistivity
and Particle Size Analysis
Resistivity as a Function of Temperature
Resistivity is determined as a function of temperature
in accordance with IEEE Standard 548. This test is conducted in
an air environment containing a specified moisture concentration.
The test is run as a function of ascending or descending temperature
or both. Data are acquired using an average ash layer electric field
of 4 kV/cm. Since relatively low applied voltage is used and no
sulfuric acid vapor is present in the environment, the values obtained
indicate the maximum ash resistivity.
Usually
the descending temperature test is suggested when no unusual
circumstances are involved. Before the test, the ash is thermally
equilibrated in dry air at 850°F for about
14 hours. It is believed that this procedure anneals the ash and
restores the surface to pre-collection condition.
If
there is a concern about the effect of combustibles, the residual
effect of a conditioning agent other than sulfuric acid vapor,
or the effect of some other agent that inhibits the reaction
of the ash with water vapor, the combination of the ascending
and descending test mode is recommended. The thermal treatment
that occurs between the two test modes is capable of eliminating
the foregoing effects. This results in ascending and descending
temperature resistivity curves that show a hysteresis related
to the presence and removal of some effect such as a significant
level of combustibles as shown in Figure
1.
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