USEPA Method 103 details the guidelines and requirements for methods
acceptable for use in determining Beryllium (Be) emissions in ducts
or stacks at stationary sources.
Particulate Be emissions are withdrawn isokinetically from three points
in a duct or stack and are collected on a filter. The collected
sample is analyzed for Be using flame atomic absorption spectrophotometry
using an air/acetylene flame or inductively coupled argon plasma (ICP)
AAS.
Guidelines for source testing are detailed in the method. These
guidelines are generally applicable; however, most sample sites differ
to some degree and temporary alterations such as stack extensions
or expansions often are required to insure the best possible sample
site. Because the total quantity of Be to be collected is quite
small, the test must be carefully conducted to prevent contamination
or loss of sample.
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